copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

Base Information

Chemical Name:copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin
CAS No.:77698-95-4
Molecular Formula:C₄₇H₃₀CuN₄O₂
Molecular Weight:746.327
Hs Code.:

Synonyms:copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

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Chemical Property of copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

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Technology Process of copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

There total 1 articles about copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 71774-36-2
copper(II) trans-meso-tetraphenyl-1-(2-ethoxycarbonylvinyl)porphyrin

: 77698-95-4
copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

Guidance literature:: With KOH; In tetrahydrofuran; ethanol; water; A soln. of complex in THF and KOH in aq. EtOH was refluxed for 12 h;; evapd., neutralized with HCl, extd. into CHCl3, dried over Na2SO4, reduced in vol., passed through silica column with CHCl3, recrystd. from CHCl3-heptane;;

Reference yield: 28.0%

: 77698-95-4
copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

: 34272-83-8
2,2,5,5-tetramethyl-3-aminopyrrolidine-1-oxyl

: 84433-35-2
copper(II) meso-tetraphenyl-2-(2-((((2,2,5,5-tetramethyl-1-oxy-4-pirrolidinyl)amino)carbonyl)amino)-trans-ethenyl)porphyrin

Guidance literature:: With sodium azide; oxalyl dichloride; In tetrahydrofuran; acetone; benzene; (COCl)2 and complex in C6H6 were stirred (2 h, room temp.), dried, dissolved in THF/acetone, added to NaN3 in H2O at 0°C, stirred (3 h, 10°C), toluene soln. was refluxed for 24 h (N2), to product in THF amine was added, refluxed for 15 h; Solvent was removed under vac., residue was chromd., recrystallyzed from CHCl3/heptane; elem. anal.;

Reference yield:

: 77698-95-4
copper(II) trans-meso-tetraphenyl-1-(3-acrylic acid)porphyrin

: copper(II) meso-tetraphenyl-2-(2-(isocyanate)-trans-ethenyl)porphyrin

Guidance literature:: With sodium azide; oxalyl dichloride; In tetrahydrofuran; acetone; benzene; (COCl)2 was added to complex in benzene, mixt. was stirred for 2 h at room temp., dried and kept for 2 h under vac., dissolved in THF/acetone, added to NaN3 in H2O (0°C), stirred for 3 h at 10°C, driedtoluene soln. refluxed for 24 h (N2); Solvent was removed under vac.; analised by IR;