(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

Base Information

Chemical Name:(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol
CAS No.:911798-10-2
Molecular Formula:C₁₁H₁₃NO₂
Molecular Weight:191.23
Hs Code.:

Synonyms:(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

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Technology Process of (4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

There total 3 articles about (4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1428235-82-8
1-methyl-1-phenylbut-3-en-1-one oxime

: 911798-10-2
(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

Guidance literature:: With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; In water; acetonitrile; tert-butyl alcohol; at 20 ℃; for 18h; Green chemistry;
DOI:10.1021/acs.orglett.6b03380

Reference yield: 19.0%

: 1221447-24-0
(E)-2-methyl-1-phenylbut-3-en-1-one oxime

: 1221447-70-6
4,5-dimethyl-3-phenyl-4,5-dihydroisoxazol-4-ol

: 911798-10-2
(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

Guidance literature:: (E)-2-methyl-1-phenylbut-3-en-1-one oxime; With 1,10-Phenanthroline; palladium diacetate; acetic acid; In water; 1,2-dichloro-ethane; at 80 ℃; under 760.051 Torr;

With potassium carbonate; In methanol; at 20 ℃; for 1h; optical yield given as %de;
DOI:10.1021/ja100716x

Reference yield:

: 504-61-0,542-72-3
(E)-but-2-enol

: 698-16-8
benzohydroximoyl chloride

: 911798-10-2
(4-methyl-3-phenyl-4,5-dihydroisoxazol-5-yl)methanol

: (5-Methyl-3-phenyl-4,5-dihydro-isoxazol-4-yl)-methanol

Guidance literature:: With L-(+)-diisopropyl tartrate; diethylzinc; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1246/cl.1993.1847