12-(benzylamino)-1-ethoxydodec-1-yne

Base Information

• Chemical Name: 12-(benzylamino)-1-ethoxydodec-1-yne
• CAS No.: 159756-55-5
• Molecular Formula: C₂₁H₃₃NO
• Molecular Weight: 315.499
• Mol file: 159756-55-5.mol

Synonyms:12-(benzylamino)-1-ethoxydodec-1-yne

Chemical Property of 12-(benzylamino)-1-ethoxydodec-1-yne

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 12-(benzylamino)-1-ethoxydodec-1-yne

There total 1 articles about 12-(benzylamino)-1-ethoxydodec-1-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H25BrO + benzylamine (100-46-9) → 12-(benzylamino)-1-ethoxydodec-1-yne (159756-55-5)

Guidance literature:

With sodium iodide; In dimethyl sulfoxide; at 55 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo9021875

Reference yield: 58.0%

12-(benzylamino)-1-ethoxydodec-1-yne (159756-55-5) → N-benzyl-2-azacyclotridecanone (41011-68-1)

Guidance literature:

In carbon dioxide; toluene; at 120 ℃; for 24h; under 241524 Torr; Supercritical conditions;

DOI:10.1021/jo9021875

Reference yield: 31.0%

12-(benzylamino)-1-ethoxydodec-1-yne (159756-55-5) → N-benzyl-2-azacyclotridecanone (41011-68-1) + C38H58N2O2 (1200405-86-2)

Guidance literature:

In carbon dioxide; at 120 ℃; for 24h; under 241524 Torr; Supercritical conditions;

DOI:10.1021/jo9021875

upstream raw materials:

benzylamine

Downstream raw materials:

N-benzyl-2-azacyclotridecanone

C₃₈H₅₈N₂O₂