dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Base Information

Chemical Name:dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate
CAS No.:220720-52-5
Molecular Formula:C₃₈H₄₂N₂O₁₀
Molecular Weight:686.759
Hs Code.:

Synonyms:dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Suppliers and Price of dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

There total 4 articles about dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 31896-88-5
benzyl 3-<2-(methoxycarbonyl)ethyl>-4-methylpyrrole-5-carboxylate

: 220720-50-3
benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

: 220720-52-5
dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Guidance literature:: With Montmorillonite clay K₁₀; In dichloromethane; Ambient temperature;
DOI:10.1021/jo9814748

Reference yield:

: 80480-42-8
methyl 4,6-dioxoheptanoate, keto-tautomer

: 220720-52-5
dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / potassium carbonate / acetone / 5 h / Heating

2: 39 percent / zinc dust, sodium acetate / acetic acid / 1 h / 90 °C

3: 94 percent / lead tetraacetate / acetic acid / 2 h / Ambient temperature

4: 83 percent / montmorillonite clay K₁₀ / CH₂Cl₂ / Ambient temperature

With lead(IV) acetate; Montmorillonite clay K₁₀; sodium acetate; potassium carbonate; zinc; In dichloromethane; acetic acid; acetone;
DOI:10.1021/jo9814748

Reference yield:

: 220720-49-0
methyl 5-<(ethoxycarbonyl)methyl>-4,6-dioxoheptanoate

: 220720-52-5
dibenzyl 3-<(ethoxycarbonyl)methyl>-3',4-bis<2-(methoxycarbonyl)ethyl>-4'-methyl-2,2'-dipyrrylmethane-5,5'-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / zinc dust, sodium acetate / acetic acid / 1 h / 90 °C

2: 94 percent / lead tetraacetate / acetic acid / 2 h / Ambient temperature

3: 83 percent / montmorillonite clay K₁₀ / CH₂Cl₂ / Ambient temperature

With lead(IV) acetate; Montmorillonite clay K₁₀; sodium acetate; zinc; In dichloromethane; acetic acid;
DOI:10.1021/jo9814748