(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Base Information

Chemical Name:(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide
CAS No.:113453-35-3
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:

Synonyms:(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Suppliers and Price of (2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Chemical Property:

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Technology Process of (2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

There total 4 articles about (2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 113453-35-3
(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / i-Pr₂EtN, Bu₄NI / tetrahydrofuran / 38 h / Ambient temperature

2: 1) O₃, Sudan III indicator, 2) Me₂S / 1) metanol, pyridine, -78 deg C; 2) room temp. 4 h

With dimethylsulfide; tetra-(n-butyl)ammonium iodide; ozone; N-ethyl-N,N-diisopropylamine; Sudan III; In tetrahydrofuran;
DOI:10.1021/ja00216a026

Reference yield:

: 113453-29-5
(2S,3R,4E)-3-hydroxy-N-methoxy-N,2-dimethyl-5-phenyl-4-pentenamide

: 113453-35-3
(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / i-Pr₂EtN, Bu₄NI / tetrahydrofuran / 38 h / Ambient temperature

2: 1) O₃, Sudan III indicator, 2) Me₂S / 1) metanol, pyridine, -78 deg C; 2) room temp. 4 h

With dimethylsulfide; tetra-(n-butyl)ammonium iodide; ozone; N-ethyl-N,N-diisopropylamine; Sudan III; In tetrahydrofuran;
DOI:10.1021/ja00216a026

Reference yield:

: 113453-28-4
<3(2S,3R,4E),4S>-3-(-3-hydroxy-2-methyl-1-oxo-5-phenyl-4-penteyl)-4-(phenylmethyl)-2-oxazolidinone

: 113453-35-3
(2S,4S)-N-methoxy-N,2-dimethyl-4-oxo-3-<(phenylmethoxy)methoxy>butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) AlMe₃ / 1) CH₂Cl₂, 30 min, room temp., toluene; 2) CH₂Cl₂, 0-10 deg C

2: 94 percent / i-Pr₂EtN, Bu₄NI / tetrahydrofuran / 38 h / Ambient temperature

3: 1) O₃, Sudan III indicator, 2) Me₂S / 1) metanol, pyridine, -78 deg C; 2) room temp. 4 h

With dimethylsulfide; trimethylaluminum; tetra-(n-butyl)ammonium iodide; ozone; N-ethyl-N,N-diisopropylamine; Sudan III; In tetrahydrofuran;
DOI:10.1021/ja00216a026