9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine

Base Information

• Chemical Name: 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine
• CAS No.: 73644-54-9
• Molecular Formula: C₂₂H₂₄ClN₅O₇
• Molecular Weight: 505.915

Synonyms:9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine

Chemical Property of 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine

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Technology Process of 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine

There total 1 articles about 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

ethyl N-benzyloxycarbonylamino-orthoacetate (13347-35-8) + 6-Chloropurine riboside (2004-06-0) → 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine (73644-54-9)

Guidance literature:

With trifluoroacetic acid; In N,N-dimethyl-formamide; for 3h; Ambient temperature;

DOI:10.1021/jm00181a015

Reference yield: 64.0%

N6-(4-aminobutyl)-2',3'-O-(methoxyethylidene)adenosine (73644-56-1) + 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine (73644-54-9) → 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N6-yl)butane (73652-50-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1021/jm00181a015

upstream raw materials:

ethyl N-benzyloxycarbonylamino-orthoacetate

6-Chloropurine riboside

Downstream raw materials:

2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

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