4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

Base Information

Chemical Name:4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl
CAS No.:1452822-65-9
Molecular Formula:C₃₁H₃₄F₂O₂
Molecular Weight:476.607
Hs Code.:

Synonyms:4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

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Technology Process of 4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

There total 8 articles about 4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1452822-26-2
(Z)-4-(3-(2-tert-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl

: 1452822-65-9
4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -80 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201203315

Reference yield:

: 842141-92-8
1-bromo-4-(3-bromo-2,2,3,3-tetrafluoropropyl)benzene

: 1452822-65-9
4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 80 °C / Schlenk technique; Inert atmosphere

3: sodium hexamethyldisilazane / tetrahydrofuran / -80 - 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hexamethyldisilazane; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; dimethyl sulfoxide; 1: |Suzuki Coupling;
DOI:10.1002/chem.201203315

Reference yield:

: 1452822-15-9
C₂₁H₂₃BrF₄O

: 1452822-65-9
4-(3-(2-tert-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 80 °C / Schlenk technique; Inert atmosphere

2: sodium hexamethyldisilazane / tetrahydrofuran / -80 - 20 °C / Inert atmosphere

With sodium hexamethyldisilazane; potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/chem.201203315