Technology Process of C71H86O10Si
There total 3 articles about C71H86O10Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
dichloromethane;
at 20 ℃;
for 1.33333h;
Molecular sieve;
DOI:10.1021/ja305864z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 1 h / 70 °C
2: borane-THF / tetrahydrofuran / 0.5 h / 20 °C
3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
4: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.33 h / 20 °C / Molecular sieve
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrapropylammonium perruthennate; borane-THF; dihydrogen peroxide; 4-methylmorpholine N-oxide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/ja305864z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: borane-THF / tetrahydrofuran / 0.5 h / 20 °C
2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
3: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.33 h / 20 °C / Molecular sieve
With
tetrapropylammonium perruthennate; borane-THF; dihydrogen peroxide; 4-methylmorpholine N-oxide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja305864z
