dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

Base Information

Chemical Name:dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate
CAS No.:1334590-63-4
Molecular Formula:C₁₈H₁₈N₂O₇S
Molecular Weight:406.416
Hs Code.:

Synonyms:dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

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Chemical Property of dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

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Technology Process of dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

There total 2 articles about dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23150-65-4
L-glutamic dimethyl ester hydrochloride

: 1334590-63-4
dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

2: piperidine; acetic acid / ethanol / 0.33 h / 150 °C / Microwave irradiation

With piperidine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide; 2: Knoevenagel condensation;
DOI:10.1016/j.ejmech.2011.05.070

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1334590-63-4
dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

2: piperidine; acetic acid / ethanol / 0.33 h / 150 °C / Microwave irradiation

With piperidine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide; 2: Knoevenagel condensation;
DOI:10.1016/j.ejmech.2011.05.070

Reference yield: 95.0%

: 1334590-63-4
dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate

: 1334590-68-9
(S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioic acid

Guidance literature:: dimethyl (S,Z)-2-(4-((2,4-dioxothiazolidin-5-ylidene)methyl)benzamido)pentanedioate; With lithium hydroxide; In methanol; water; at 20 ℃; for 15h;

With hydrogenchloride; In water; pH=2;
DOI:10.1016/j.ejmech.2011.05.070