C₃₄H₄₆N₂O₅Si

Base Information

• Chemical Name: C₃₄H₄₆N₂O₅Si
• CAS No.: 130253-29-1
• Molecular Formula: C₃₄H₄₆N₂O₅Si
• Molecular Weight: 590.835
• Mol file: 130253-29-1.mol

Synonyms:C₃₄H₄₆N₂O₅Si

Chemical Property of C₃₄H₄₆N₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₄₆N₂O₅Si

There total 1 articles about C₃₄H₄₆N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

t-butyldimethylsiyl triflate (69739-34-0) → C34H46N2O5Si (130253-29-1)

Guidance literature:

With osmium(VIII) oxide; In tetrahydrofuran; pyridine;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield: 92.0%

C34H46N2O5Si (130253-29-1) → C34H48N2O5Si (130253-41-7)

Guidance literature:

With sodium tetrahydroborate; In methanol;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

C34H46N2O5Si (130253-29-1) → C26H28N2O3 (130253-44-0)

Guidance literature:

Multi-step reaction with 15 steps

1: 92 percent / NaBH₄ / methanol

2: 83 percent / NaIO₄ / methanol

3: 78 percent / NaBH₄ / propan-2-ol; H₂O; CH₂Cl₂ / -20 °C

4: 96 percent / pyridine

5: 100 percent / n-Bu₄NF / tetrahydrofuran

6: 90 percent / CH₂Cl₂

7: 68 percent / Pb(OAc)4 / CH₂Cl₂ / -70 °C

8: AcOH / tetrahydrofuran; H₂O / Ambient temperature

9: 80 percent / NaBH₄ / methanol / 0 °C

10: 80 percent / Et₃N / CH₂Cl₂

11: 90 percent / aq. KOH / methanol

12: 93 percent / Et₃N, DMAP / CH₂Cl₂

13: 66 percent / H₂ / Pd-C / acetic acid; ethanol

14: 90 percent / n-Bu₄NF / tetrahydrofuran

15: MgO / H₂O; tetrahydrofuran

With pyridine; lead(IV) acetate; dmap; potassium hydroxide; sodium tetrahydroborate; sodium periodate; tetrabutyl ammonium fluoride; hydrogen; magnesium oxide; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; isopropyl alcohol;

DOI:10.1016/S0040-4039(00)88787-0

upstream raw materials:

t-butyldimethylsiyl triflate

Downstream raw materials:

C₃₄H₄₈N₂O₅Si

C₂₈H₃₂N₂O₅

C₃₂H₄₄N₂O₄Si

C₂₉H₃₄N₂O₅