C₁₅H₁₆N₂O₄S₂

Base Information

Chemical Name:C₁₅H₁₆N₂O₄S₂
CAS No.:1170193-92-6
Molecular Formula:C₁₅H₁₆N₂O₄S₂
Molecular Weight:352.435
Hs Code.:

C<sub>15</sub>H<sub>16</sub>N<sub>2</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₁₅H₁₆N₂O₄S₂

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Chemical Property of C₁₅H₁₆N₂O₄S₂

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Technology Process of C₁₅H₁₆N₂O₄S₂

There total 5 articles about C₁₅H₁₆N₂O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1170193-84-6
C₁₅H₁₅NO₄S₂

: 1170193-92-6
C₁₅H₁₆N₂O₄S₂

Guidance literature:: C₁₅H₁₅NO₄S₂; With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

With hydrogenchloride; In methanol; water; at 20 ℃;
DOI:10.1016/j.bmcl.2013.01.120

Reference yield:

: 100063-22-7
methyl 3-amino-5-phenylthiophene-2-carboxylate

: 1170193-92-6
C₁₅H₁₆N₂O₄S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium nitrate; sulfur dioxide; hydrogenchloride / water

1.2: 0 °C

2.1: ammonia / 1,4-dioxane / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

4.1: triphenylphosphine; carbon tetrabromide / tetrahydrofuran; dichloromethane / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 55 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 60 °C

7.1: sodium hydroxide / water; methanol / 20 °C

8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate; triethylamine / N,N-dimethyl-formamide / 20 °C

8.2: 20 °C

With hydrogenchloride; sodium nitrate; lithium aluminium tetrahydride; carbon tetrabromide; sulfur dioxide; ammonia; sodium hydride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.01.120

Reference yield:

: 113387-58-9
5-phenyl-3-chlorosulfonyl-2-methoxycarbonyl thiophene

: 1170193-92-6
C₁₅H₁₆N₂O₄S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonia / 1,4-dioxane / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

3.1: triphenylphosphine; carbon tetrabromide / tetrahydrofuran; dichloromethane / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 55 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 60 °C

6.1: sodium hydroxide / water; methanol / 20 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate; triethylamine / N,N-dimethyl-formamide / 20 °C

7.2: 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; ammonia; sodium hydride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.01.120