dodeca-1,11-dien-6-yne

Base Information

• Chemical Name: dodeca-1,11-dien-6-yne
• CAS No.: 524069-92-9
• Molecular Formula: C₁₂H₁₈
• Molecular Weight: 162.275
• Mol file: 524069-92-9.mol

Synonyms:dodeca-1,11-dien-6-yne

Chemical Property of dodeca-1,11-dien-6-yne

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of dodeca-1,11-dien-6-yne

There total 1 articles about dodeca-1,11-dien-6-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

hept-1-en-6-yne (65939-59-5) + bromopentene (1119-51-3) → dodeca-1,11-dien-6-yne (524069-92-9)

Guidance literature:

hept-1-en-6-yne; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.75h;

bromopentene; In tetrahydrofuran;

DOI:10.1039/b209889j

Reference yield: 67.0%

[Ti(OC6H3Ph2-2,6)2Cl2] (110300-61-3) + dodeca-1,11-dien-6-yne (524069-92-9) → (OC6H3(C6H5)2)2Ti(CH2CH(CH2)3C)2

Guidance literature:

With Na/Hg; In not given; recrystd. (benzene);

DOI:10.1039/b209889j

Reference yield: 48.0%

N,N'-dimethyl-N,N'-diphenylguanidine (46893-81-6) + dodeca-1,11-dien-6-yne (524069-92-9) → 4-[(1E)-hexa-1,5-dien-1-yl]-N,1-dimethyl-4-pent-4-en-1-yl-N-phenyl-1,4-dihydroquinazolin-2-amine

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; silver(I) acetate; In isopropyl alcohol; at 60 ℃; for 8h;

DOI:10.1039/c5cc06388d

upstream raw materials:

hept-1-en-6-yne

bromopentene