2'-(acetoxymethyl)-6'-nitrophenacyl acetate

Base Information

Chemical Name:2'-(acetoxymethyl)-6'-nitrophenacyl acetate
CAS No.:157989-01-0
Molecular Formula:C₁₃H₁₃NO₇
Molecular Weight:295.249
Hs Code.:

Synonyms:2'-(acetoxymethyl)-6'-nitrophenacyl acetate

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Chemical Property of 2'-(acetoxymethyl)-6'-nitrophenacyl acetate

Chemical Property:

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Technology Process of 2'-(acetoxymethyl)-6'-nitrophenacyl acetate

There total 4 articles about 2'-(acetoxymethyl)-6'-nitrophenacyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4127-55-3
2'-methyl-6'-nitroacetophenone

: 157989-01-0
2'-(acetoxymethyl)-6'-nitrophenacyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / N-bromosuccinimide, benzoyl peroxide / benzene / 12 h / Heating

2: 62 percent / acetic acid / 4 h / 100 °C

3: bromine / acetic acid / 1.3 h / 70 °C

4: dimethylsulfoxide / 2.5 h / 80 °C

With N-Bromosuccinimide; Perbenzoic acid; bromine; In acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1021/jm00045a007

Reference yield:

: 157988-99-3
2'-(bromomethyl)-6'-nitroacetophenone

: 157989-01-0
2'-(acetoxymethyl)-6'-nitrophenacyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / acetic acid / 4 h / 100 °C

2: bromine / acetic acid / 1.3 h / 70 °C

3: dimethylsulfoxide / 2.5 h / 80 °C

With bromine; In acetic acid; dimethyl sulfoxide;
DOI:10.1021/jm00045a007

Reference yield:

: 157989-00-9
2'-(acetoxymethyl)-6'-nitroacetophenone

: 157989-01-0
2'-(acetoxymethyl)-6'-nitrophenacyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / acetic acid / 1.3 h / 70 °C

2: dimethylsulfoxide / 2.5 h / 80 °C

With bromine; In acetic acid; dimethyl sulfoxide;
DOI:10.1021/jm00045a007