N,N-Tetramethylene-5-iodo-2-phenylpentenamide

Base Information

Chemical Name:N,N-Tetramethylene-5-iodo-2-phenylpentenamide
CAS No.:152667-57-7
Molecular Formula:C₁₅H₂₀INO
Molecular Weight:357.234
Hs Code.:

Synonyms:N,N-Tetramethylene-5-iodo-2-phenylpentenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Tetramethylene-5-iodo-2-phenylpentenamide

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Technology Process of N,N-Tetramethylene-5-iodo-2-phenylpentenamide

There total 2 articles about N,N-Tetramethylene-5-iodo-2-phenylpentenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76403-12-8
2-Phenyl-4-pentenoyl chloride

: 152667-57-7
N,N-Tetramethylene-5-iodo-2-phenylpentenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) cyclohexene, BH₃*SMe₂, 2.) NaOAc, ICl / 1.) THF, 0 deg C, 1 h; room temp., 1 h, 2.) MeOH, 0 deg C, 1 h

With pyridine; dimethylsulfide borane complex; sodium acetate; Iodine monochloride; cyclohexene; In dichloromethane;
DOI:10.1021/jo00077a053

Reference yield:

: 152667-64-6
2-phenyl-1-(pyrrolidin-1-yl)pent-4-en-1-one

: 152667-57-7
N,N-Tetramethylene-5-iodo-2-phenylpentenamide

Guidance literature:: With dimethylsulfide borane complex; sodium acetate; Iodine monochloride; cyclohexene; Yield given. Multistep reaction; 1.) THF, 0 deg C, 1 h; room temp., 1 h, 2.) MeOH, 0 deg C, 1 h;
DOI:10.1021/jo00077a053