1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

Base Information

Chemical Name:1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline
CAS No.:1539295-26-5
Molecular Formula:C₅H₉NO₂*C₂₃H₂₅NO₅
Molecular Weight:510.587
Hs Code.:

Synonyms:1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

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Chemical Property of 1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

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Technology Process of 1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

There total 23 articles about 1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₃₁H₃₃NO₉

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 1539295-26-5
1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

Guidance literature:: C₃₁H₃₃NO₉; With water; sodium hydroxide; In 2-methyltetrahydrofuran; at 50 ℃; for 3h;

L-proline; In water; isopropyl alcohol; at 23 ℃; for 4h;

Reference yield:

: 2-(4-cyclopropylbenzyl)-4-((2S,3R,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)benzonitrile

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 1539295-26-5
1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

Guidance literature:: In ethanol; water; at 20 ℃; for 16h;

Reference yield:

: 946525-36-6
2-(phenoxymethyl)-4-(2,3,4,6-tetra-O-acetyl-1-deoxy-D-glucopyranos-1-yl)-benzonitrile

: 1539295-26-5
1-cyano-2-(4-cyclopropylbenzyl)-4-(β-D-glucopyranos-1-yl)benzene L-proline

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide; acetic anhydride; acetic acid / 6 h / 55 °C

2.1: potassium carbonate; palladium dichloride / acetone; water / 16 h / 20 °C / Cooling with ice

2.2: 1 h / 20 °C

3.1: water; ethanol / 16 h / 20 °C

With hydrogen bromide; acetic anhydride; potassium carbonate; acetic acid; palladium dichloride; In ethanol; water; acetone;