C₂₂H₂₉NO₃

Base Information

Chemical Name:C₂₂H₂₉NO₃
CAS No.:1417544-00-3
Molecular Formula:C₂₂H₂₉NO₃
Molecular Weight:355.477
Hs Code.:

C<sub>22</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₂H₂₉NO₃

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Chemical Property of C₂₂H₂₉NO₃

Chemical Property:

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Technology Process of C₂₂H₂₉NO₃

There total 6 articles about C₂₂H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1417543-99-7
C₂₂H₂₅NO₃

: 1417544-00-3
C₂₂H₂₉NO₃

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; under 760.051 Torr;
DOI:10.1016/j.bmc.2012.10.060

Reference yield:

: 1227951-58-7
N-[3-(2-hydroxy-5-methoxyphenyl)propyl]propionamide

: 1417544-00-3
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic anhydride; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 24 h / 70 °C / Inert atmosphere

3: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; triethylamine; trifluoroacetic anhydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.10.060

Reference yield:

: 1227951-37-2
3-(2-benzyloxy-5-methoxyphenyl)propylamine

: 1417544-00-3
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: 5%-palladium/activated carbon; hydrogen / methanol / 24 h

3: trifluoroacetic anhydride; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 24 h / 70 °C / Inert atmosphere

5: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 5%-palladium/activated carbon; palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; triethylamine; trifluoroacetic anhydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.10.060