(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

Base Information

Chemical Name:(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester
CAS No.:1242185-45-0
Molecular Formula:C₂₉H₂₈N₄O₅
Molecular Weight:512.565
Hs Code.:

Synonyms:(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

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Chemical Property of (4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

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Technology Process of (4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

There total 1 articles about (4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

: 1012860-26-2
N-allyl-2-[(3R)-3-(hydroxymethyl)-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-1-yl]acetamide

: 5416-93-3
4-Methoxyphenyl isocyanate

: 1242185-45-0
(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.06.010

Reference yield: 81.0%

: 1242185-45-0
(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: (R)-methyl 4-(2-(3-((4-methoxyphenylcarbamoyloxy)methyl)-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-1-yl)acetamido)but-2-enoate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 100 ℃; for 2h; Microwave irradiation;
DOI:10.1016/j.bmc.2010.06.010

Reference yield: 77.0%

: 1242185-45-0
(4-methoxy-phenyl)-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylmethyl ester

: 140-88-5,9003-32-1
ethyl acrylate

: 1402828-79-8
C₃₂H₃₂N₄O₇

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1002/cmdc.201200274