(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

Base Information

Chemical Name:(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene
CAS No.:623148-35-6
Molecular Formula:C₁₆H₁₈O₅
Molecular Weight:290.316
Hs Code.:

Synonyms:(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

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Chemical Property of (1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

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Technology Process of (1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

There total 1 articles about (1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 93382-48-0
allyl 4,6-O-benzylidene-α-D-glucopyranoside

: 623148-35-6
(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

Guidance literature:: allyl 4,6-O-benzylidene-α-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With N-tosylimidazole; In N,N-dimethyl-formamide; at 50 ℃; for 4.5h;
DOI:10.1021/ol0490678

Reference yield: 92.0%

: 623148-35-6
(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

: 1210898-25-1
C₁₆H₁₉N₃O₅

Guidance literature:: With sodium azide; water; ammonium chloride; In ethyl methyl ether; Reflux;
DOI:10.1055/s-0029-1218525

Reference yield: 78.0%

: 623148-35-6
(1aS,2S,3aR,6R,7aR,7bS)-2-Allyloxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

: (1aS,3aR,6R,7aR,7bS)-6-Phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalen-2-ol

Guidance literature:: With palladium diacetate; diethylamine; triphenylphosphine; In methanol; dichloromethane; at 20 ℃; for 4.5h;
DOI:10.1021/ol0490678