1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

Base Information

Chemical Name:1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate
CAS No.:1167416-16-1
Molecular Formula:C₂₆H₃₀ClN₃O₄
Molecular Weight:483.995
Hs Code.:

Synonyms:1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

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Chemical Property of 1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

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Technology Process of 1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

There total 1 articles about 1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1167416-14-9
3-[2-(aminomethyl)-6-(5-{3-chloro-4-[(1-methylethyl)oxy] phenyl}-1,2,4-oxadiazol-3-yl)phenyl]-1-propanol

: 1167416-16-1
1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

Guidance literature:: 3-[2-(aminomethyl)-6-(5-{3-chloro-4-[(1-methylethyl)oxy] phenyl}-1,2,4-oxadiazol-3-yl)phenyl]-1-propanol; With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 20 ℃; for 2h;

di-tert-butyl dicarbonate; With dmap; In dichloromethane; for 2h;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1167416-16-1
1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

: 1167416-17-2
[6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepin-2-yl]acetic acid

: 1167416-15-0
1,1-dimethylethyl [6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepin-2-yl]acetate

Guidance literature:: 1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

With ammonia; In methanol;

bromoacetic acid tert-butyl ester; With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1167416-16-1
1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate

: 1167415-55-5
[6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepin-2-yl]acetic acid hydrochloride

Guidance literature:: 1,1-dimethylethyl 6-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1,3,4,5-tetrahydro-2H-2-benzazepine-2-carboxylate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

With ammonia; In methanol;

bromoacetic acid tert-butyl ester; With hydrogenchloride; potassium carbonate; more than 3 stages;