3-(decanoylamino)-4-methoxy-N-phenylbenzamide

Base Information

Chemical Name:3-(decanoylamino)-4-methoxy-N-phenylbenzamide
CAS No.:6496-05-5
Molecular Formula:C₁₃H₁₇N
Molecular Weight:187.285
Hs Code.:
DSSTox Substance ID:DTXSID80409471

Synonyms:6496-05-5;ST50986953;DTXSID80409471;AKOS024358068

Suppliers and Price of 3-(decanoylamino)-4-methoxy-N-phenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-(decanoylamino)-4-methoxy-N-phenylbenzamide

Chemical Property:

Vapor Pressure:7.41E-11mmHg at 25°C
Boiling Point:518.6°Cat760mmHg
Flash Point:267.4°C
Density:1.109g/cm³
XLogP3:6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:12
Exact Mass:396.24129289
Heavy Atom Count:29
Complexity:477

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCC(=O)NC1=C(C=CC(=C1)C(=O)NC2=CC=CC=C2)OC

Technology Process of 3-(decanoylamino)-4-methoxy-N-phenylbenzamide

There total 9 articles about 3-(decanoylamino)-4-methoxy-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-1,2,3,6,11,11a-Hexahydro-4H-pyrido[1,2-b]isoquinolin-4-one

: 6496-05-5
(S)-1,3,4,6,11,11a-Hexahydro-2H-pyrido[1,2-b]isoquinoline

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Reflux;
DOI:10.1007/s00706-018-2244-5

Reference yield:

: 1232683-35-0
(S)-5-amino-6-(2-hydroxymethylphenyl)hexan-1-ol

: 6496-05-5
(S)-1,3,4,6,11,11a-Hexahydro-2H-pyrido[1,2-b]isoquinoline

Guidance literature:: (S)-5-amino-6-(2-hydroxymethylphenyl)hexan-1-ol; With thionyl chloride; In chloroform; at 0 - 50 ℃;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 10h;
DOI:10.1002/ejoc.201000111

Reference yield:

: (S)-1,2,3,11a-tetrahydro-4H-pyrido[1,2-b]isoquinoline-4,11(6H)-dione

: 6496-05-5
(S)-1,3,4,6,11,11a-Hexahydro-2H-pyrido[1,2-b]isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate; methanol / 0 °C

2.1: sodium hydride; 1H-imidazole / tetrahydrofuran; mineral oil / 0.5 h / Reflux; Inert atmosphere

2.2: 0.75 h / Reflux; Inert atmosphere

2.3: 0.5 h / Reflux; Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 1 h / Inert atmosphere; Reflux

4.1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

With 1H-imidazole; methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1007/s00706-018-2244-5