2-bromo-4-fluorophenyl dimethylcarbamate

Base Information

Chemical Name:2-bromo-4-fluorophenyl dimethylcarbamate
CAS No.:1380586-38-8
Molecular Formula:C₉H₉BrFNO₂
Molecular Weight:262.078
Hs Code.:

Synonyms:2-bromo-4-fluorophenyl dimethylcarbamate

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Chemical Property of 2-bromo-4-fluorophenyl dimethylcarbamate

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Technology Process of 2-bromo-4-fluorophenyl dimethylcarbamate

There total 2 articles about 2-bromo-4-fluorophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 7541-20-0
O-(4-fluorophenyl)-N,N-dimethylcarbamate

: 1380586-38-8
2-bromo-4-fluorophenyl dimethylcarbamate

Guidance literature:: With N-Bromosuccinimide; silver hexafluoroantimonate; copper diacetate; [Cp^A₅RhCl₂]₂; In 1,2-dichloro-ethane; at 20 ℃; for 18h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.202000253

Reference yield:

: 371-41-5
4-Fluorophenol

: 1380586-38-8
2-bromo-4-fluorophenyl dimethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 5 h / Inert atmosphere; Reflux

2: N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid / 1,2-dichloro-ethane / 16 h / 60 - 90 °C / Inert atmosphere

With N-Bromosuccinimide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jo300713h