1-(4-fluorophenyl)vinylphosphonic acid

Base Information

Chemical Name:1-(4-fluorophenyl)vinylphosphonic acid
CAS No.:1159205-39-6
Molecular Formula:C₈H₈FO₃P
Molecular Weight:202.122
Hs Code.:

Synonyms:1-(4-fluorophenyl)vinylphosphonic acid

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Chemical Property of 1-(4-fluorophenyl)vinylphosphonic acid

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Technology Process of 1-(4-fluorophenyl)vinylphosphonic acid

There total 1 articles about 1-(4-fluorophenyl)vinylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 403-42-9
1-(4-fluorophenyl)ethanone

: 1159205-39-6
1-(4-fluorophenyl)vinylphosphonic acid

Guidance literature:: 1-(4-fluorophenyl)ethanone; With phosphorus trichloride; at 0 - 20 ℃; for 3h;

With acetic acid; at 10 ℃;

With hydrogenchloride; In water; for 3h; Reflux;
DOI:10.1021/ja305780z

Reference yield: 94.0%

: 1159205-39-6
1-(4-fluorophenyl)vinylphosphonic acid

: (S)-(1-(4-fluorophenyl)ethyl)phosphonic acid

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; C₃₂H₄₅FeNOP₂; hydrogen; In ethanol; at 20 ℃; for 6h; under 7600.51 Torr; enantioselective reaction; Glovebox; Autoclave;
DOI:10.1021/acs.orglett.7b02098

Reference yield:

: 1159205-39-6
1-(4-fluorophenyl)vinylphosphonic acid

: (-)-(1-(4-fluorophenyl)ethyl)phosphonic acid

Guidance literature:: 1-(4-fluorophenyl)vinylphosphonic acid; With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; C₂₉H₂₅N₂O₄P; hydrogen; In dichloromethane; at 20 ℃; for 12h; under 7500.75 Torr; optical yield given as %ee; enantioselective reaction; Autoclave;
DOI:10.1021/ja305780z