methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside

Base Information

• Chemical Name: methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside
• CAS No.: 634606-89-6
• Molecular Formula: C₂₉H₄₉NO₇Si₂
• Molecular Weight: 579.882

Synonyms:methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside

Chemical Property of methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside

There total 2 articles about methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ²-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

benzonitrile oxide (873-67-6) + methyl 4-O-acryloyl-2,3-di-O-t-butyldimethylsilyl-6-deoxy-α-D-glucopyranoside (347384-19-4) → methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ2-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside (634606-89-6)

Guidance literature:

In dichloromethane; at 20 ℃; for 4h;

DOI:10.1055/s-2003-41404

Reference yield:

methyl 6-deoxy-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside (347384-33-2) → methyl 6-deoxy-4-O-[(5R)-3-phenyl-Δ2-isoxazoline-5-carbonyl]-2,3-di-O-t-butyldimethylsilyl-α-D-glucopyranoside (634606-89-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

2: 96 percent / CH₂Cl₂ / 4 h / 20 °C

With triethylamine; In dichloromethane;

DOI:10.1055/s-2003-41404

upstream raw materials:

benzonitrile oxide

methyl 4-O-acryloyl-2,3-di-O-t-butyldimethylsilyl-6-deoxy-α-D-glucopyranoside

methyl 6-deoxy-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

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