2-[p-(Dimethylamino)phenyl]-1-phenylcyclopropanecarbonitrile

Base Information

• Chemical Name: 2-[p-(Dimethylamino)phenyl]-1-phenylcyclopropanecarbonitrile
• CAS No.: 6114-58-5
• Molecular Formula: C₁₈H₁₈N₂
• Molecular Weight: 262.354
• Hs Code.: 2926909090
• Mol file: 6114-58-5.mol

Synonyms:Cyclopropanecarbonitrile,2-[p-(dimethylamino)phenyl]-1-phenyl- (7CI,8CI)

Chemical Property of 2-[p-(Dimethylamino)phenyl]-1-phenylcyclopropanecarbonitrile

Chemical Property:

• Vapor Pressure: 1.65E-07mmHg at 25°C
• Boiling Point: 427.3°Cat760mmHg
• Flash Point: 185.7°C
• PSA: 27.03000
• Density: 1.13g/cm³
• LogP: 3.70148

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[p-(Dimethylamino)phenyl]-1-phenylcyclopropanecarbonitrile

There total 3 articles about 2-[p-(Dimethylamino)phenyl]-1-phenylcyclopropanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

trimethylsulfoxonium iodide (1774-47-6) + phenylacetonitrile (140-29-4) + 4-dimethylamino-benzaldehyde (100-10-7) → (1R,2R)-2-(4-(dimethylamino)phenyl)-1-phenylcyclopropanecarbonitrile (6114-58-5,22370-60-1,83688-81-7)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.333333h; diastereoselective reaction;

DOI:10.1021/jo302443k

Reference yield:

→ (1R,2R)-2-(4-(dimethylamino)phenyl)-1-phenylcyclopropanecarbonitrile (6114-58-5,22370-60-1,83688-81-7)

Guidance literature:

/BRN= 216861/, CH2N2;

DOI:10.1016/S0040-4020(01)92807-8

Reference yield:

→ 1-Cyano-1-phenyl-2-(p-dimethylaminophenyl)-cyclopropan (6114-58-5)

Guidance literature:

aus trans-4-Dimethylamino-α-cyanostilben;

upstream raw materials:

trimethylsulfoxonium iodide

phenylacetonitrile

4-dimethylamino-benzaldehyde

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