dithioessigsaeure-methylester

Base Information

Chemical Name:dithioessigsaeure-methylester
CAS No.:135394-37-5
Molecular Formula:C₁₁H₁₃NS₃
Molecular Weight:255.429
Hs Code.:

<Methylphenylamino(thiocarbonyl)>dithioessigsaeure-methylester

Synonyms:dithioessigsaeure-methylester

Suppliers and Price of dithioessigsaeure-methylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dithioessigsaeure-methylester

Chemical Property:

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Technology Process of dithioessigsaeure-methylester

There total 3 articles about dithioessigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 135394-34-2
N,N,S-Trimethyl-3-(methylphenylamino)propinamidium-iodid

: 135394-37-5
dithioessigsaeure-methylester

Guidance literature:: With pyridine; hydrogen sulfide; In tetrahydrofuran; at -50 ℃;

Reference yield:

: 4231-31-6
N-methyl N-phenylamino acetylene

: 135394-37-5
dithioessigsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / Et₃N, CuI, PPh₃ / PdCl₂*2PPh₃ / Ambient temperature

2: 90 percent / CH₂Cl₂ / 12 h / Ambient temperature

3: 67 percent / H₂S, pyridine / tetrahydrofuran / -50 °C

With pyridine; copper(l) iodide; hydrogen sulfide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 135394-25-1
N,N-Dimethyl-3-(methylphenylamino)propinthioamid

: 135394-37-5
dithioessigsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 67 percent / H₂S, pyridine / tetrahydrofuran / -50 °C

With pyridine; hydrogen sulfide; In tetrahydrofuran; dichloromethane;