3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

Base Information

Chemical Name:3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate
CAS No.:1418224-99-3
Molecular Formula:C₃₉H₃₃N₂P₂*F₆P
Molecular Weight:736.616
Hs Code.:

Synonyms:3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

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Chemical Property of 3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

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Technology Process of 3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

There total 2 articles about 3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 1418224-90-4
3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium chloride

: 1418224-99-3
3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

Guidance literature:: With thallium(I) hexafluorophosphate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/om301230f

Reference yield:

: 158363-40-7
N¹,N²-bis(2-(diphenylphosphanyl)phenyl)ethane-1,2-diamine

: 1418224-99-3
3-bis(o-diphenylphosphino)phenyl-1H-imidazolinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / tetrahydrofuran; diethyl ether / 1 h / Inert atmosphere

1.2: 12 h / 120 °C / Inert atmosphere; Reflux

2.1: thallium(I) hexafluorophosphate / dichloromethane / 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; thallium(I) hexafluorophosphate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/om301230f