C₅₇H₆₀O₁₂Si

Base Information

Chemical Name:C₅₇H₆₀O₁₂Si
CAS No.:950682-32-3
Molecular Formula:C₅₇H₆₀O₁₂Si
Molecular Weight:965.182
Hs Code.:

C<sub>57</sub>H<sub>60</sub>O<sub>12</sub>Si

Synonyms:C₅₇H₆₀O₁₂Si

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Chemical Property of C₅₇H₆₀O₁₂Si

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Technology Process of C₅₇H₆₀O₁₂Si

There total 11 articles about C₅₇H₆₀O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₈O₈

: 950682-32-3
C₅₇H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 99 percent / TPAP; NMO; MS 4A / CH₂Cl₂

2.1: H₂O; Dowex 50W-X₈ / methanol / 50 °C

3.1: Et₃N / CH₂Cl₂

4.1: 100 percent / H₂ / Pd(OH)2/C / ethyl acetate; methanol

5.1: TMSOTf; MS 4A / acetonitrile / -40 °C

5.2: 66 percent / Et₃N / CH₂Cl₂

6.1: 68 percent / EDCI; DMAP; TsOH*H₂O / CH₂Cl₂ / 20 °C

7.1: K₂CO₃; pyridine / 120 °C

7.2: Et₃N / CH₂Cl₂

8.1: DDQ; H₂O / CH₂Cl₂

9.1: pyridine

With pyridine; dmap; N-methyl-2-indolinone; tetrapropylammonium perruthennate; trimethylsilyl trifluoromethanesulfonate; Dowex 50W-X₈; water; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dihydroxide; In methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2007.06.134

Reference yield:

: 950682-24-3
C₂₇H₄₂O₅Si₂

: 950682-32-3
C₅₇H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / H₂ / Pd(OH)2/C / ethyl acetate; methanol

2.1: TMSOTf; MS 4A / acetonitrile / -40 °C

2.2: 66 percent / Et₃N / CH₂Cl₂

3.1: 68 percent / EDCI; DMAP; TsOH*H₂O / CH₂Cl₂ / 20 °C

4.1: K₂CO₃; pyridine / 120 °C

4.2: Et₃N / CH₂Cl₂

5.1: DDQ; H₂O / CH₂Cl₂

6.1: pyridine

With pyridine; dmap; trimethylsilyl trifluoromethanesulfonate; water; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dihydroxide; In methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2007.06.134

Reference yield:

: C₂₁H₂₆O₈

: 950682-32-3
C₅₇H₆₀O₁₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: H₂O; Dowex 50W-X₈ / methanol / 50 °C

2.1: Et₃N / CH₂Cl₂

3.1: 100 percent / H₂ / Pd(OH)2/C / ethyl acetate; methanol

4.1: TMSOTf; MS 4A / acetonitrile / -40 °C

4.2: 66 percent / Et₃N / CH₂Cl₂

5.1: 68 percent / EDCI; DMAP; TsOH*H₂O / CH₂Cl₂ / 20 °C

6.1: K₂CO₃; pyridine / 120 °C

6.2: Et₃N / CH₂Cl₂

7.1: DDQ; H₂O / CH₂Cl₂

8.1: pyridine

With pyridine; dmap; trimethylsilyl trifluoromethanesulfonate; Dowex 50W-X₈; water; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dihydroxide; In methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2007.06.134