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2-(azidomethyl)-3-(phenylethynyl)thiophene

Base Information
  • Chemical Name:2-(azidomethyl)-3-(phenylethynyl)thiophene
  • CAS No.:1083167-27-4
  • Molecular Formula:C13H9N3S
  • Molecular Weight:239.301
  • Hs Code.:
2-(azidomethyl)-3-(phenylethynyl)thiophene

Synonyms:2-(azidomethyl)-3-(phenylethynyl)thiophene

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Chemical Property of 2-(azidomethyl)-3-(phenylethynyl)thiophene
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Technology Process of 2-(azidomethyl)-3-(phenylethynyl)thiophene

There total 1 articles about 2-(azidomethyl)-3-(phenylethynyl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 14h;
DOI:10.1021/ja805326f
Guidance literature:
With N-chloro-succinimide; boron trifluoride diethyl etherate; In acetonitrile; at 60 ℃; for 2h;
DOI:10.1002/adsc.202101169
Guidance literature:
With iodine; sodium hydrogencarbonate; In nitromethane; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja805326f
upstream raw materials:

C13H10OS

Downstream raw materials:

4-iodo-5-phenylthieno[2,3-c]pyridine

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