4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione

Base Information

• Chemical Name: 4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione
• CAS No.: 82253-68-7
• Molecular Formula: C₂₅H₁₈Cl₂O₃
• Molecular Weight: 437.322

Synonyms:4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione

Chemical Property of 4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione

Chemical Property:

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Technology Process of 4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione

There total 1 articles about 4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.0^2,7>undeca-4,9-diene-3,6,11-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone (26307-17-5) + 2,3-dichloro-1,4-benzoquinone (5145-42-6) → 4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.02,7>undeca-4,9-diene-3,6,11-trione (82253-68-7)

Guidance literature:

In benzene; for 0.25h; Heating;

DOI:10.1016/0040-4020(81)80021-X

Reference yield: 90.0%

4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.02,7>undeca-4,9-diene-3,6,11-trione (82253-68-7) → C25H18Cl2O3

Guidance literature:

for 0.75h; Inert atmosphere; Photolysis;

Reference yield: 90.0%

4,5-dichloro-1,8-dimethyl-9,10-diphenyl-tricyclo<6.2.1.02,7>undeca-4,9-diene-3,6,11-trione (82253-68-7) → C25H18Cl2O3 (82266-70-4)

Guidance literature:

In benzene; for 0.75h; Irradiation;

DOI:10.1016/0040-4020(81)80021-X

upstream raw materials:

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone

2,3-dichloro-1,4-benzoquinone

Downstream raw materials:

C₂₅H₁₈Cl₂O₃

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