benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

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Chemical Name:benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate
CAS No.:1041482-32-9
Molecular Formula:C₂₄H₂₇N₃O₄
Molecular Weight:421.496
Hs Code.:

Synonyms:benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

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Chemical Property of benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

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Technology Process of benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

There total 3 articles about benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1041482-26-1
dibenzyl (2,2-dimethylpent-4-en-1-yl)amino-methylylidenebiscarbamate

: 1041482-32-9
benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

Guidance literature:: With palladium diacetate; potassium carbonate; copper(ll) bromide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1039/b719479j

Reference yield:

: 73604-46-3
2,2-dimethyl-1-amino-pent-4-ene

: 1041482-32-9
benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

2: trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene / acetonitrile / 5 h / -48 °C / Inert atmosphere; Schlenk technique

With trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201403891

Reference yield:

: 2978-30-5
2,2-dimethylpent-4-enenitrile

: 1041482-32-9
benzyl 3-(benzyloxycarbonylimino)-6,6-dimethyltetrahydro-1H-pyrrolo[1,2-c]imidazole-2(3H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 16 h / 0 - 25 °C / Inert atmosphere; Schlenk technique

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

3: trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene / acetonitrile / 5 h / -48 °C / Inert atmosphere; Schlenk technique

With lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene; triethylamine; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/chem.201403891