bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

Base Information

Chemical Name:bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide
CAS No.:342595-50-0
Molecular Formula:C₂₀H₁₄F₁₂O₂S₂Se
Molecular Weight:657.403
Hs Code.:

Synonyms:bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

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Chemical Property of bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

Chemical Property:

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Technology Process of bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

There total 3 articles about bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 684-16-2
Hexafluoroacetone

: 342595-54-4
(phenylthio)methyl 3,3,3-trifluoro-2-hydroxy-1-(phenyl-thio)-2-(trifluoromethyl)propyl selenide

: 342595-50-0
bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

: bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

Guidance literature:: (phenylthio)methyl 3,3,3-trifluoro-2-hydroxy-1-(phenyl-thio)-2-(trifluoromethyl)propyl selenide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

Hexafluoroacetone; In tetrahydrofuran; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1039/b009789f

Reference yield:

: 7205-91-6
phenylthiomethyl chloride

: 342595-50-0
bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 91 percent / Na₂Se / tetrahydrofuran / 12 h / 25 °C

2.1: LDA / tetrahydrofuran / 0.17 h / -78 °C

2.2: 28 percent / tetrahydrofuran / 0.5 h / -78 °C

3.1: LDA / tetrahydrofuran / 0.17 h / -78 °C

3.2: 61 percent / tetrahydrofuran / 0.5 h / -78 °C

With sodium selenide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1039/b009789f

Reference yield:

: 342595-52-2
bis[(phenylthio)methyl] selenide

: 342595-50-0
bis[3,3,3-trifluoro-2-hydroxy-1-(phenylthio)-2-(trifluoromethyl)propyl] selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 0.17 h / -78 °C

1.2: 28 percent / tetrahydrofuran / 0.5 h / -78 °C

2.1: LDA / tetrahydrofuran / 0.17 h / -78 °C

2.2: 61 percent / tetrahydrofuran / 0.5 h / -78 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1039/b009789f