1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole

Base Information

• Chemical Name: 1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole
• CAS No.: 1026658-72-9
• Molecular Formula: C₂₀H₂₁N₃O₄
• Molecular Weight: 367.404

Synonyms:1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole

Chemical Property of 1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole

Chemical Property:

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Technology Process of 1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole

There total 1 articles about 1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitroresorcinol monomethyl ether (3114-61-2) + 1-(3-chloropropyl)-5-methyl-4-phenylimidazole (141815-91-0) → 1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole (1026658-72-9)

Guidance literature:

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

DOI:10.1021/jm00063a014

Reference yield:

1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole (1026658-72-9) → N-[6-Methoxy-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl) propoxy}]phenyl-N'-pentylurea

Guidance literature:

Multi-step reaction with 2 steps

1: zinc, AcOH / 1 h

2: CHCl₃ / 12 h / Heating

With acetic acid; zinc; In chloroform;

DOI:10.1021/jm00063a014

Reference yield:

1-[3-(3-Methoxy-2-nitro-phenoxy)-propyl]-5-methyl-4-phenyl-1H-imidazole (1026658-72-9) → 2-Methoxy-6-[3-(5-methyl-4-phenyl-imidazol-1-yl)-propoxy]-phenylamine (149353-19-5)

Guidance literature:

With acetic acid; zinc; for 1h;

DOI:10.1021/jm00063a014

upstream raw materials:

2-nitroresorcinol monomethyl ether

1-(3-chloropropyl)-5-methyl-4-phenylimidazole

Downstream raw materials:

2-Methoxy-6-[3-(5-methyl-4-phenyl-imidazol-1-yl)-propoxy]-phenylamine

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