chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

Base Information

• Chemical Name: chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾
• CAS No.: 82839-15-4
• Molecular Formula: C₁₁H₆ClO₅PW
• Molecular Weight: 468.442

Synonyms:chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

Chemical Property of chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

There total 3 articles about chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

diethylaminophenylphosphine-pentacarbonyl-tungsten(0)=Diethylaminophenylphosphin-pentacarbonyl-wolfram(0) (82839-12-1) → chlorophenylphosphine-pentacarbonyl-tungsten(0)=Chlorophenylphosphin-pentacarbonyl-wolfram(0) (82839-15-4)

Guidance literature:

With hydrogenchloride; In pentane; byproducts: Et2NH*HCl; (Ar); addn. of gaseous HCl under stirring at 0°C; removal of solvent in vac. at room temp.; digered with pentane; filtn.; dried in vac.; chromy. (silica gel/pentane); elem. anal.; IR; (31)P NMR; mass spectra;

DOI:10.1016/0022-328X(90)85169-Y

Reference yield: 74.0%

C6H5(C6H5NH)PHW(CO)5 (82839-10-9) → chlorophenylphosphine-pentacarbonyl-tungsten(0)=Chlorophenylphosphin-pentacarbonyl-wolfram(0) (82839-15-4)

Guidance literature:

With hydrogenchloride; In toluene; gas. anhydrous HCl bubbled through toluene soln. of W complex for 5 minat room temp., mixture cooled to 0°C; filtration, evapn., recrystn. (hexane); elem. anal.;

Reference yield: 30.0%

{NEt4}{HW(CO)5} (80907-47-7) + Dichlorophenylphosphine (644-97-3) → chlorophenylphosphine-pentacarbonyl-tungsten(0)=Chlorophenylphosphin-pentacarbonyl-wolfram(0) (82839-15-4)

Guidance literature:

In dichloromethane; byproducts: Et4NCl; room temp.;

DOI:10.1021/om00140a031

upstream raw materials:

C₆H₅(C₆H₅NH)PHW(CO)5

{NEt₄}{HW(CO)5}

Dichlorophenylphosphine

diethylaminophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Diethylaminophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

Downstream raw materials:

phenylphosphine pentacarbonyltungsten⁽⁰⁾

PhPCl₂W(CO)5

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 82839-15-4 chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

Send

Send

Metric Ton KG G Pound L ML

Send

Send