C₄₅H₈₄O₅Si₄

Base Information

• Chemical Name: C₄₅H₈₄O₅Si₄
• CAS No.: 1328886-38-9
• Molecular Formula: C₄₅H₈₄O₅Si₄
• Molecular Weight: 817.501
• Mol file: 1328886-38-9.mol

Synonyms:C₄₅H₈₄O₅Si₄

Chemical Property of C₄₅H₈₄O₅Si₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₅H₈₄O₅Si₄

There total 6 articles about C₄₅H₈₄O₅Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C52H90O5Si4 (1328886-30-1) → C45H84O5Si4 (1328886-38-9)

Guidance literature:

With 20 % Pd(OH)2/C; hydrogen; In ethyl acetate; at 20 ℃; for 24h;

DOI:10.1055/s-0030-1260586

Reference yield:

C37H52O5Si → C45H84O5Si4 (1328886-38-9)

Guidance literature:

Multi-step reaction with 3 steps

1: water; acetic acid / 1.5 h / 20 °C

2: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C

3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C

With 2,6-dimethylpyridine; 20 % Pd(OH)2/C; water; hydrogen; acetic acid; In dichloromethane; ethyl acetate;

DOI:10.1055/s-0030-1260586

Reference yield:

C42H56O6Si → C45H84O5Si4 (1328886-38-9)

Guidance literature:

Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / tetrahydrofuran / 20 °C

2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane

3: water; acetic acid / 1.5 h / 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C

5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C

With 2,6-dimethylpyridine; 20 % Pd(OH)2/C; water; hydrogen; pyridinium p-toluenesulfonate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; ethyl acetate;

DOI:10.1055/s-0030-1260586

upstream raw materials:

C₄₅H₆₀O₆Si

C₃₄H₄₈O₅Si

C₅₂H₉₀O₅Si₄

t-butyldimethylsiyl triflate

Downstream raw materials:

C₄₅H₈₂O₅Si₄

C₄₈H₈₈O₄S₂Si₄