C₃₃H₃₉N₇O₁₀S

Base Information

Chemical Name:C₃₃H₃₉N₇O₁₀S
CAS No.:1429313-34-7
Molecular Formula:C₃₃H₃₉N₇O₁₀S
Molecular Weight:725.78
Hs Code.:

C<sub>33</sub>H<sub>39</sub>N<sub>7</sub>O<sub>10</sub>S

Synonyms:C₃₃H₃₉N₇O₁₀S

Suppliers and Price of C₃₃H₃₉N₇O₁₀S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₉N₇O₁₀S

Chemical Property:

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Technology Process of C₃₃H₃₉N₇O₁₀S

There total 8 articles about C₃₃H₃₉N₇O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1429313-33-6
C₂₆H₃₄BrN₇O₈S

: 25487-66-5
3-Carboxyphenylboronic acid

: 1429313-34-7
C₃₃H₃₉N₇O₁₀S

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; XPhos; In 1,4-dioxane; water; at 80 ℃; for 5h; Inert atmosphere;

Reference yield:

: 214000-16-5
N-(tert-butoxycarbonyl)-N'-(2-nitrobenzenesulfonyl)ethylenediamine

: 1429313-34-7
C₃₃H₃₉N₇O₁₀S

Guidance literature:: Multi-step reaction with 8 steps

1: caesium carbonate / N,N-dimethyl-formamide / 50 °C

2: water; sodium hydroxide / methanol / 1.5 h / 20 °C

3: acetyl chloride / 2 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / Reflux

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere

6: hydrazine / ethanol / Reflux

7: dmap / tetrahydrofuran / 20 °C

8: XPhos; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 5 h / 80 °C / Inert atmosphere

With dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; water; caesium carbonate; N-ethyl-N,N-diisopropylamine; acetyl chloride; triphenylphosphine; sodium hydroxide; hydrazine; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1429313-28-9
C₁₅H₂₃N₃O₇S

: 1429313-34-7
C₃₃H₃₉N₇O₁₀S

Guidance literature:: Multi-step reaction with 6 steps

1: acetyl chloride / 2 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / Reflux

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere

4: hydrazine / ethanol / Reflux

5: dmap / tetrahydrofuran / 20 °C

6: XPhos; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 5 h / 80 °C / Inert atmosphere

With dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; acetyl chloride; triphenylphosphine; hydrazine; XPhos; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetonitrile;