tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

Base Information

Chemical Name:tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate
CAS No.:1256550-67-0
Molecular Formula:C₃₀H₃₈O₁₂
Molecular Weight:590.625
Hs Code.:

Synonyms:tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

Chemical Property:

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Technology Process of tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

There total 4 articles about tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1304014-13-8
tri(tert-butyl) (2R,3S)-2-(2,2,4,4-tetraisopropylbenzo[f][1,3,5,2,4]trioxadisilepin-7-yl)chroman-3,5,7-triyl tricarbonate

: 1256550-67-0
tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ol200808q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1256550-67-0
tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C

With dmap; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol200808q

Reference yield:

: 1304014-12-7
(2R,3S)-2-(2,2,4,4-tetraisopropylbenzo[f][1,3,5,2,4]trioxadisilepin-7-yl)chroman-3,5,7-triol

: 1256550-67-0
tri(tert-butyl) (2R,3S)-2-(3,4-dihydroxyphenyl)chroman-3,5,7-triyl tricarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C

With dmap; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol200808q