1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

Base Information

Chemical Name:1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde
CAS No.:1335139-24-6
Molecular Formula:C₁₆H₂₈N₂O₂Si
Molecular Weight:308.496
Hs Code.:

Synonyms:1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

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Chemical Property of 1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

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Technology Process of 1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

There total 3 articles about 1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335139-21-3
[1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazol-4-yl]methanol

: 1335139-24-6
1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydrogencarbonate; In dichloromethane; water; toluene; at 20 ℃; for 12h;

Reference yield:

: 1335139-23-5
C₁₈H₃₂N₂O₃Si

: 1335139-24-6
1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene; dichloromethane / 12 h / 20 °C

With lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; toluene;

Reference yield:

: 690992-74-6
trans-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}cyclohexanamine

: 1335139-24-6
1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-imidazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 12 h / 85 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

3: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene; dichloromethane / 12 h / 20 °C

With lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; toluene;