Technology Process of C36H50O7
There total 3 articles about C36H50O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
at 20 ℃;
for 1h;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C
2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
2.2: 1.5 h / 50 °C
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
2.1: |Yamaguchi Lactonization / 2.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
1.2: 1.5 h / 50 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C
With
2,4,6-trichlorobenzoyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water; toluene;
1.1: |Yamaguchi Lactonization / 1.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
