N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

Base Information

Chemical Name:N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride
CAS No.:1608474-80-1
Molecular Formula:C₁₇H₂₀FNO₄*ClH
Molecular Weight:357.809
Hs Code.:

Synonyms:N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

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Chemical Property of N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

Chemical Property:

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Technology Process of N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

There total 4 articles about N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1608474-79-8
N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylaniline

: 1608474-80-1
N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

Guidance literature:: With hydrogenchloride; In methanol; diethyl ether; at 20 ℃; for 1.16667h;
DOI:10.1016/j.ejmech.2014.03.032

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1608474-80-1
N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 5 h / 100 °C / Sealed tube; Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

3: hydrogenchloride / methanol; diethyl ether / 1.17 h / 20 °C

With hydrogenchloride; palladium diacetate; sodium hydride; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.032

Reference yield:

: C₁₆H₁₈FNO₄

: 1608474-80-1
N-(3-fluoro-4-methoxyphenyl)-3,4,5-trimethoxy-N-methylbenzenaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

2: hydrogenchloride / methanol; diethyl ether / 1.17 h / 20 °C

With hydrogenchloride; sodium hydride; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.032