(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

Base Information

Chemical Name:(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol
CAS No.:161346-04-9
Molecular Formula:C₂₂H₃₂O₄
Molecular Weight:360.494
Hs Code.:

Synonyms:(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

Suppliers and Price of (1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

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Technology Process of (1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

There total 4 articles about (1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 161284-40-8
(1R)-1-C-(cyclopenta-1',3'-dienyl)-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

: 161346-04-9
(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

Guidance literature:: With hydrogen; palladium on activated charcoal; In hexane; for 14h; Ambient temperature;
DOI:10.1002/hlca.19940770620

Reference yield: 95.0%

: 161284-38-4
(1R)-1-C-(cyclopenta-1',4'-dienyl)-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

: 161346-04-9
(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

Guidance literature:: With hydrogen; palladium on activated charcoal; In hexane; for 14h; Ambient temperature;
DOI:10.1002/hlca.19940770620

Reference yield:

: 50866-82-5
2,3:4,5-di-O-isopropylidene-aldehydo-D-ribose

: 161346-04-9
(1R)-1-C-cyclopentyl-1-deoxy-2,3:4,5-di-O-isopropylidene-1-C-phenyl-D-ribitol

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) Et₃N, Ac₂O, DMAP / 1.) THF, -100 deg C, 0.5 h; 2.) THF, rt, 1.5 h

2: cyclohexane; diethyl ether / 0.5 h / -78 °C

3: 95 percent / H₂ / 10percent Pd/C / hexane / 14 h / Ambient temperature

With dmap; hydrogen; acetic anhydride; triethylamine; palladium on activated charcoal; In diethyl ether; hexane; cyclohexane;
DOI:10.1002/hlca.19940770620