2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

Base Information

Chemical Name:2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)
CAS No.:1442741-99-2
Molecular Formula:C₅₁H₈₂N₆O₈
Molecular Weight:907.247
Hs Code.:

Synonyms:2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

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Technology Process of 2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

There total 7 articles about 2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1235584-97-0
3,4-bis((2-ethylhexyl)oxy)benzoic acid

: 104274-80-8
2,2-bis(azidomethyl)propan-1,3-diol

: 1442741-99-2
2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

Guidance literature:: With S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja403323y

Reference yield:

: 1235584-96-9
methyl 3,4-bis((2-ethylhexyl)oxy)benzoate

: 1442741-99-2
2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol; water / 2 h / Reflux

1.2: pH 1

2.1: dicyclohexyl-carbodiimide; S-phenyl 4-methoxybenzenesulfinothioate / dichloromethane / 12 h / 25 °C / Inert atmosphere

With S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide; potassium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1021/ja403323y

Reference yield:

: 3296-90-0
bis(bromomethyl)bis(hydroxymethyl)methane

: 1442741-99-2
2,2-bis(azidomethyl)propane-1,3-diyl bis(3,4-bis((2-ethyloctyl)oxy)benzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 16 h / 110 °C / Inert atmosphere

2: dicyclohexyl-carbodiimide; S-phenyl 4-methoxybenzenesulfinothioate / dichloromethane / 12 h / 25 °C / Inert atmosphere

With sodium azide; S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja403323y