1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

Base Information

Chemical Name:1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene
CAS No.:1314875-97-2
Molecular Formula:C₇₁H₇₁N₃O₈
Molecular Weight:1094.36
Hs Code.:

Synonyms:1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

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Chemical Property of 1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

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Technology Process of 1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

There total 1 articles about 1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 180206-32-0
2,3,4-tris(benzyloxy)benzoic acid

: 149525-65-5
1,3,5-triethyl-2,4,6-tris(aminomethyl)benzene

: 1314875-97-2
1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

Guidance literature:: 2,3,4-tris(benzyloxy)benzoic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; for 1h;

1,3,5-triethyl-2,4,6-tris(aminomethyl)benzene; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 95.0%

: 1314875-97-2
1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

: 172089-14-4
1-(9H-fluoren-9-yl)-3,19-dioxo-2,8,11,14-tetraoxa-4,18-diazadocosan-22-oic acid

: 1314875-98-3
1-N-[(13'-Fmoc-amino-4',7',10'-trioxatridecyl)succinamoyl]aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzoylaminomethyl)-2,4,6-triethylbenzene

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 1314875-97-2
1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene

: 16526-68-4
cis-1,3,5-cyclohexane tricarboxylic acid

: cis-N₁,N₃,N₅-tris[3,5-bis(2,3,4-trihydroxybenzamidomethyl)-2,4,6-triethylphenylmethyl]-1,3,5-cyclohexanetricarboxamide

Guidance literature:: cis-1,3,5-cyclohexane tricarboxylic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In dichloromethane; for 0.0833333h;

1-aminomethyl-3,5-bis(2,3,4-tribenzyloxybenzamidomethyl)-2,4,6-triethylbenzene; With triethylamine; In dichloromethane; at 20 ℃; for 2h;

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; at 30 ℃; under 760.051 Torr;
DOI:10.1016/j.ejmech.2015.10.027