5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

Base Information

Chemical Name:5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride
CAS No.:126950-52-5
Molecular Formula:C₃₀H₃₀OP*Cl
Molecular Weight:472.994
Hs Code.:

Synonyms:5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

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Chemical Property of 5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

Chemical Property:

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Technology Process of 5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

There total 2 articles about 5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126950-49-0
P-isopropyl-P-phenyldibenzophospholium iodide

: 126950-52-5
5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / diethyl ether / 6 h / Ambient temperature

2: 2.) methanolic HCl / 1.) ether, -78 deg C, 15 min, 2.) -78 deg C

With hydrogenchloride; sodium amide; In diethyl ether;
DOI:10.1021/ja00166a026

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 126950-50-3
5-Isopropylidene-5-phenyl-5H-5λ⁵-dibenzophosphole

: 126950-52-5
5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) ether, -78 deg C, 15 min, 2.) -78 deg C;
DOI:10.1021/ja00166a026

Reference yield:

: 126950-52-5
5-(2-Hydroxy-1,1-dimethyl-4-phenyl-butyl)-5-phenyl-5H-dibenzophospholium; chloride

: 126950-51-4,127061-15-8
C₃₀H₂₉OP

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -109 ℃; Product distribution; Mechanism; other bases, solvents, and temperatures;
DOI:10.1021/ja00166a026