16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

Base Information

Chemical Name:16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate
CAS No.:82210-67-1
Molecular Formula:C₃₁H₄₂O₇S
Molecular Weight:558.736
Hs Code.:

Synonyms:16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

Chemical Property:

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Technology Process of 16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

There total 3 articles about 16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

: 72204-67-2
16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate

: 98-59-9
p-toluenesulfonyl chloride

: 82210-67-1
16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

Guidance literature:: With pyridine; for 24h; Ambient temperature;

Reference yield:

: 88168-34-7
16-acetoxymethylene-3β-acetoxy-5-androstene-17-one

: 82210-67-1
16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / ethanol / 24 h / 0 °C

2: pyridine / 0 °C

3: 93.2 percent / pyridine / 24 h / Ambient temperature

With pyridine; sodium tetrahydroborate; In ethanol;

Reference yield:

: 56910-00-0
16α-hydroxymethylandrost-5-ene-3β,17β-diol 3-acetate

: 82210-67-1
16α-acetoxymethyl-5-androstene-3β,17β-diol 3-acetate 17-p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0 °C

2: 93.2 percent / pyridine / 24 h / Ambient temperature

With pyridine;