C₆₁H₉₇N₅O₁₅Si

Base Information

Chemical Name:C₆₁H₉₇N₅O₁₅Si
CAS No.:345664-75-7
Molecular Formula:C₆₁H₉₇N₅O₁₅Si
Molecular Weight:1168.55
Hs Code.:

C<sub>61</sub>H<sub>97</sub>N<sub>5</sub>O<sub>15</sub>Si

Synonyms:C₆₁H₉₇N₅O₁₅Si

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Chemical Property of C₆₁H₉₇N₅O₁₅Si

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Technology Process of C₆₁H₉₇N₅O₁₅Si

There total 20 articles about C₆₁H₉₇N₅O₁₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 345664-75-7
C₆₁H₉₇N₅O₁₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: 1.204 g / 2,6-lutidine / CH₂Cl₂ / 2.5 h / 0 - 20 °C

2: NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 0.5774 g / dicyclohexylcarbodiimide; 4-dimethylaminopyridine / toluene / 0 - 20 °C

4: morpholine / Pd(PPh₃)4 / tetrahydrofuran / 20 °C

5: 0.2315 g / EDAC*HCl; 4-dimethylaminopyridine / CH₂Cl₂ / 4.5 h / 0 - 20 °C

6: 96 percent / ethyldiisopropylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 - 20 °C

7: magnesium bromide diethyl etherate / CH₂Cl₂ / 6 h / 0 - 20 °C

With morpholine; 2,6-dimethylpyridine; dmap; sodium hydroxide; magnesium bromide ethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ol9910058

Reference yield:

: 126587-61-9
Z-leucylprolyl-N,O-dimethyltyrosine-O-Boc-threonine-OSEM

: 345664-75-7
C₆₁H₉₇N₅O₁₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂ / Pd/C / methanol; ethyl acetate / 5 h

2: 96 percent / ethyldiisopropylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 - 20 °C

3: magnesium bromide diethyl etherate / CH₂Cl₂ / 6 h / 0 - 20 °C

With dmap; hydrogen; magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ol9910058

Reference yield:

: 17407-55-5
(S)-2-Hydroxy-3-methylbutanoic acid

: 345664-75-7
C₆₁H₉₇N₅O₁₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / anhydrous potassium carbonate; tetrabutylammonium iodide / dimethylformamide / 1 h / 20 °C

2: 0.5774 g / dicyclohexylcarbodiimide; 4-dimethylaminopyridine / toluene / 0 - 20 °C

3: morpholine / Pd(PPh₃)4 / tetrahydrofuran / 20 °C

4: 0.2315 g / EDAC*HCl; 4-dimethylaminopyridine / CH₂Cl₂ / 4.5 h / 0 - 20 °C

5: 96 percent / ethyldiisopropylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 - 20 °C

6: magnesium bromide diethyl etherate / CH₂Cl₂ / 6 h / 0 - 20 °C

With morpholine; dmap; tetra-(n-butyl)ammonium iodide; potassium carbonate; magnesium bromide ethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol9910058