1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one

Base Information

• Chemical Name: 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one
• CAS No.: 130750-11-7
• Molecular Formula: C₁₆H₂₅N₃O₂
• Molecular Weight: 291.393

Synonyms:1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one

Chemical Property of 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one

Chemical Property:

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Technology Process of 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one

There total 2 articles about 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionic acid ethyl ester (130750-10-6) → 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one (130750-11-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; 0 deg C to room temperature;

DOI:10.1016/0040-4039(90)80084-Y

Reference yield:

(S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionaldehyde (130750-12-8) → 1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one (130750-11-7)

Guidance literature:

With sodium tetrahydroborate; In ethanol; Ambient temperature;

DOI:10.1016/0040-4039(90)80084-Y

Reference yield: 90.0%

1,3-Diethyl-5-((S)-1-hydroxymethyl-2-phenyl-ethyl)-[1,3,5]triazinan-2-one (130750-11-7) → (S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionaldehyde (130750-12-8)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;

DOI:10.1016/0040-4039(90)80084-Y

upstream raw materials:

(S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionaldehyde

(S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionic acid ethyl ester

Downstream raw materials:

(S)-2-(3,5-Diethyl-4-oxo-[1,3,5]triazinan-1-yl)-3-phenyl-propionaldehyde

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