methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

Base Information

Chemical Name:methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate
CAS No.:1218782-00-3
Molecular Formula:C₁₄H₂₀NO₆P
Molecular Weight:329.29
Hs Code.:

Synonyms:methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

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Chemical Property of methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

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Technology Process of methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

There total 1 articles about methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 78553-47-6
methyl (2S)-2-[N-(benzyloxycarbonyl)amino]pent-4-enoate

: 1218782-00-3
methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); hypophosphorous acid; In methanol; water; at 80 ℃; for 5h;
DOI:10.1021/jm901523t

Reference yield: 67.0%

: 1218782-00-3
methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1218782-06-9
methyl (4S)-3-[((4-(N-benzyloxycarbonyl)amino-4-methoxycarbonyl)butyl)(hydroxy)phosphinyl]propanoate

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm901523t

Reference yield:

: 1218782-00-3
methyl (2S)-2-(N-benzyloxycarbonyl)amino-5-[(hydroxy)phosphinyl]pentanoate

: 22042-71-3
(4-formylphenoxy)acetic acid

: [(4S)-4-(N-benzyloxycarbonyl)amino-4-methoxycarbonylpropyl][(4-hydroxy-5-methoxy-3-nitrophenyl)hydroxymethyl]phosphinic acid

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.7b01438