methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

Base Information

Chemical Name:methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate
CAS No.:443683-45-2
Molecular Formula:C₁₇H₁₇NO₅S
Molecular Weight:347.392
Hs Code.:

Synonyms:methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

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Technology Process of methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

There total 3 articles about methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 77378-24-6
(prop-2-ynyloxy)acetic acid chloride

: 443683-36-1
methyl (2R,4R)-2-benzoylthiazolidine-4-carboxylate

: 443683-45-2
methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo010807p

Reference yield: 41.0%

: 77378-24-6
(prop-2-ynyloxy)acetic acid chloride

: 443683-37-2
methyl (2S,4R)-2-benzoylthiazolidine-4-carboxylate

: 443683-45-2
methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo010807p

Reference yield:

: 1074-12-0
phenylglyoxal hydrate

: 443683-45-2
methyl (2R,4R)-2-benzoyl-N-(prop-2-ynyloxyacetyl)thiazolidine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogen carbonate / ethanol / 20 °C

2: 41 percent / anhydrous potassium carbonate / CH₂Cl₂ / 18 h / 20 °C

With potassium carbonate; potassium hydrogencarbonate; In ethanol; dichloromethane;
DOI:10.1021/jo010807p