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C36H40O4Si

Base Information
  • Chemical Name:C36H40O4Si
  • CAS No.:1092804-24-4
  • Molecular Formula:C36H40O4Si
  • Molecular Weight:564.797
  • Hs Code.:
C<sub>36</sub>H<sub>40</sub>O<sub>4</sub>Si

Synonyms:C36H40O4Si

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Chemical Property of C36H40O4Si
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Technology Process of C36H40O4Si

There total 15 articles about C36H40O4Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
Guidance literature:
Multi-step reaction with 15 steps
1.1: water; acetic acid / 16 h / 20 °C
2.1: sodium periodate / 1,4-dioxane; water / 1.67 h
3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice
4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C
5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C
6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C
6.2: 16.33 h / -78 - 20 °C
7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C
7.2: 4 h / 50 °C
8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C
8.2: 0.5 h
9.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C
9.2: 2 h / -78 °C
10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C
11.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C
12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C
13.1: hydrogenchloride
14.1: dmap
15.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride
With hydrogenchloride; dmap; sodium periodate; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
Guidance literature:
Multi-step reaction with 13 steps
1.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice
2.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C
4.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C
4.2: 16.33 h / -78 - 20 °C
5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C
5.2: 4 h / 50 °C
6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C
6.2: 0.5 h
7.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C
7.2: 2 h / -78 °C
8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C
9.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C
10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C
11.1: hydrogenchloride
12.1: dmap
13.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride
With hydrogenchloride; dmap; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; sodium hydride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
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