methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

Base Information

Chemical Name:methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate
CAS No.:1030607-29-4
Molecular Formula:C₄₄H₇₄O₆Si₃
Molecular Weight:783.324
Hs Code.:

methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

Synonyms:methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

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Chemical Property of methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

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Technology Process of methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

There total 1 articles about methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1030607-48-7
(1S,2S,3R,4S,5S)-2-((1,3-dithian-2-yl)methyl)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethylcyclopentanecarboxylate

: 1030607-29-4
methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

Guidance literature:: With calcium carbonate; methyl iodide; In water; acetonitrile; at 20 ℃; for 40h;
DOI:10.1021/ol800419v

Reference yield: 47.0%

: 28075-51-6
cyclohept-1-en-1-yl trifluoromethanesulfonate

: 1030607-29-4
methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate

: 1161082-91-2
C₅₀H₈₂O₅Si₃

Guidance literature:: cyclohept-1-en-1-yl trifluoromethanesulfonate; methyl (1S,2S,3R,4S,5S)-3-(tert-butyldimethylsilyloxy)-5-((5S,7S)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecan-5-yl)-2,4-dimethyl-2-(2-oxoethyl)cyclopentanecarboxylate; With chromium dichloride; nickel dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 30h;

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.3987/COM-08-S(D)2